Actual problems in dentistry Actual problems in dentistry Проблемы стоматологии 2077-7566 2412-9461 57962 10.18481/2077-7566-2023-19-1-126-132 ОРТОПЕДИЧЕСКАЯ СТОМАТОЛОГИЯ ORTHOPEDIC DENTISTRY ОРТОПЕДИЧЕСКАЯ СТОМАТОЛОГИЯ QUANTITATIVE ASSESSMENT OF DENTAL PROSTHETIC FLUORESCENCE МЕТОДИКА КОЛИЧЕСТВЕННОЙ ОЦЕНКИ ФЛУОРЕСЦЕНЦИИ ЗУБОПРОТЕЗНЫХ МАТЕРИАЛОВ Брандт Николай Николаевич Brandt Nikolay Nikolaevich brandt@physics.msu.ru

кандидат физико-математических наук;

candidate of physical and mathematical sciences;

 Вердиян Самвел Арменович Verdiyan Samvel Armenovich samvelverdiyan@gmail.com Лебеденко Степан Игоревич Lebedenko Stepan Igorevich si@lasi.ru

кандидат физико-математических наук;

candidate of physical and mathematical sciences;

 Саркисян Мартирос Сергеевич Sarkisyan Martiros Sergeevich Sarkisyan_ms@pfur.ru

доктор медицинских наук;

doctor of medical sciences;

 Лебеденко Игорь Юльевич Lebedenko Igor' Yul'evich lebedenkoi@mail.ru

доктор медицинских наук;

doctor of medical sciences;

 Московский государственный университет имени М. В. Ломоносова Москва Россия M.V. Lomonosov Moscow State University Moscow Russian Federation Российского университета дружбы народов имени Патриса Лумумбы Москва Россия Peoples' Friendship University of Russia named after Patrice Lumumba Moscow Russian Federation ООО «Клиника Боско» Москва Россия Bosco Clinic LLC Moscow Russian Federation Российского университета дружбы народов имени Патриса Лумумбы Москва Россия Peoples' Friendship University of Russia named after Patrice Lumumba Moscow Russian Federation Российского университета дружбы народов имени Патриса Лумумбы Москва Россия Peoples' Friendship University of Russia named after Patrice Lumumba Moscow Russian Federation 22 05 2023 22 05 2023 19 1 126 132 29 03 2023 https://dental-press.ru/en/nauka/article/57962/view

Предмет. При возбуждении ультрафиолетовым излучением естественные зубы флуоресцируют в синей спектральной области, поэтому в состав используемых в стоматологической практике композитных материалов и стеклокерамики добавляют флуоресцирующие компоненты. Керамика на основе диоксида циркония может флуоресцировать за счёт нанесения глазурей, красителей или флуоресцентных паст. Однако методики количественного определения интенсивности флуоресценции зубопротезных материалов на сегодняшний день отсутствуют. Цель –– разработка методики количественного определения интенсивности флуоресценции зубопротезных материалов. Методология. Исследования проводились на физическом факультете МГУ. Спектры флуоресценции измерялись на специально созданной экспериментальной установке на основе волоконно-оптического спектрофлуориметра Ocean Optics. Математическая обработка экспериментальных данных выполнялась с помощью программного продукта Origin. В качестве образцов использовались керамические заготовки из диоксида циркония «Ziceram T» A2 отечественного производства без покрытия и с нанесением флуоресцентной глазури «Ivocolor fluo», а также натуральные зубы пациентов. Результаты. Измерены спектры флуоресценции серии образцов натуральных зубов и зубных протезов из диоксида циркония с различным числом нанесённых слоёв флуоресцентной глазури. Интенсивность флуоресценции образцов диоксида циркония линейно возрастает при увеличении числа слоёв глазури. Выводы. Предложена методика количественного определения интенсивности флуоресценции натуральных зубов и зубопротезных материалов. Спектр флуоресценции образца может быть охарактеризован предложенным в работе параметром флуоресценции Ф. Интенсивность флуоресценции зубного протеза на основе диоксида циркония может быть увеличена до значения, соответствующего натуральному зубу, путём нанесения на протез заданного числа слоёв флуоресцентной глазури.

Subject. Ceramics based on zirconia can fluoresce through the additional application of fluorescent glazes, fluorescent dyes, as well. To date, there are no methods for assessing the fluorescence of dental materials used in prosthetics. The aim –– Development of a method for quantitative determination of the fluorescence intensity of dental prosthetic materials. Methodology. The study was conducted in the laboratory of the Faculty of Physics of Moscow State University. Fluorescence was excited by an ultraviolet lamp. The fluorescence spectra of the samples were measured using the Ocean Optics fiber optic spectrofluorometer. Ceramic billets made of zirconia "Ziceram T" A2 of domestic production without and with the staining of fluorescent glaze "Ivocolor fluo", as well as natural teeth were used as samples for patients. Results. Samples of domestic zirconia acquire fluorescent properties after applying and sintering the fluorescent glaze. The varied number of layers of the applied glaze explains why the fluorescence intensity increases. The authors compare the fluorescence spectra of two natural teeth with the spectra of zirconia samples with two and three layers of glaze. The spectra coincide well with each other in pairs. A fluorescence spectrum that is similar to one of the natural tooth samples can thus be achieved by varying the number of glaze layers. Conclusions. The analysis of the fluorescence spectra of samples of zirconia from domestic production after application and sintering of fluorescent glaze shows a similar fluorescence spectrum to samples of natural teeth.

 спектрофлуориметрия флуоресценция зубы диоксид циркония флуоресцентные глазури Spectrofluorometry fluorescence fluorescence of teeth zirconia fluorescence fluorescent glaze

Дьяконенко Е.Е., Вердиян С.А., Сахабиева Д.А., Лебеденко И.Ю. Флуоресценция стоматологических керамических материалов на основе диоксида циркония. Стоматология. 2021;100(3):109-114. [Dyakonenko EE, Verdiyan SA, Sakhabieva DA, Lebedenko IYu. Fluorescence of zirconia-based dental ceramic materials. Stomatologiya. 2021;100(3):109-114.] (In Russ.) https://doi.org/10.17116/stomat2021100031109 С.А.Горбань, Е.А. Михалева, В.Н. Полтанов, В.И. Степкин, В.П.Чуев, Воссоздание эффекта флуоресценции в стоматологической керамике «Ультропалин» Современная ортопедическая стоматология 2014;21:71-74. [S.A.Gorban, E.A. Mikhaleva, V.N. Poltanov, V.I. Stepkin, V.P. Chuev, Reconstruction of the fluorescence effect in dental ceramics "Ultropalin" Modern orthopedic dentistry 2014;21:71-74.] (In Russ.) Iñaki Gamborena, Markus B. Blatz The Gray Zone Around Dental Implants: Keys to Esthetic Success. The American journal of esthetic dentistry volume 2011;1 26-46 Iñaki Gamborena, Markus B. 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ISSN:1659-1046. 23 Takashi nakamura, Shinya Okamura, Hisataka Nishida, Hirofumi Usami, Yoshiro Nakano, Kazumichi Wakabayashi, Tohru Sekino and Hirofumi Yatani Fluorescence of thulium-doped translucent zirconia Dental Materials Journal 2018;37:1010-1016 doi:10.4012/dmj.2017-384 Takashi nakamura, Shinya Okamura, Hisataka Nishida, Hirofumi Usami, Yoshiro Nakano, Kazumichi Wakabayashi, Tohru Sekino and Hirofumi Yatani Fluorescence of thulium-doped translucent zirconia Dental Materials Journal 2018;37:1010-1016 doi:10.4012/dmj.2017-384 Claudia Angela Maziero Volpato; Filipe Samuel Silva; Filipe Samuel Silva Fluorescence of natural teeth and restorative materials, methods for analysis and quantification: A literature review J Esthet Restor Dent. 2018;30: 397- 407. 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Fluorescence of thulium-doped translucent zirconia // Dental Materials Journal. - 2018;37:1010-1016. doi:10.4012/dmj.2017-384 Claudia Angela Maziero Volpato, Filipe Samuel Silva, Filipe Samuel Silva. Fluorescence of natural teeth and restorative materials, methods for analysis and quantification: A literature review // J Esthet Restor Dent. - 2018;30:397-407. DOI: 10.1111/jerd.12421 Claudia Angela Maziero Volpato, Filipe Samuel Silva, Filipe Samuel Silva. Fluorescence of natural teeth and restorative materials, methods for analysis and quantification: A literature review // J Esthet Restor Dent. - 2018;30:397-407. DOI: 10.1111/jerd.12421 Arndt Happe, Verena Schulte-Mattler, Christian Strassert, Michael Naumann, Michael Stimmelmayr, Joachim E. Zöller, Daniel Rothamel. In Vitro Color Changes of Soft Tissues Caused by Dyed Fluorescent Zirconia and Nondyed, Nonfluorescent Zirconia in Thin Mucosa // Int J Periodontics Restorative Dent. - 2013;33:e1-e8. doi: 10.11607/prd.1303 Arndt Happe, Verena Schulte-Mattler, Christian Strassert, Michael Naumann, Michael Stimmelmayr, Joachim E. Zöller, Daniel Rothamel. In Vitro Color Changes of Soft Tissues Caused by Dyed Fluorescent Zirconia and Nondyed, Nonfluorescent Zirconia in Thin Mucosa // Int J Periodontics Restorative Dent. - 2013;33:e1-e8. doi: 10.11607/prd.1303 Caroline Freitas Rafael, Paulo Francisco Cesar, Marcio Frede, Ricardo de Souza Magini, Anja Liebermann, Claudia Angela Maziero Volpato. Impact of laboratory treatment with coloring and fluorescent liquids on the optical properties of zirconia before and after accelerated aging // The Journal of Prosthetic Dentistry. - 2018;120:276-281. DOI: 10.1016/j.prosdent.2017.10.017 Caroline Freitas Rafael, Paulo Francisco Cesar, Marcio Frede, Ricardo de Souza Magini, Anja Liebermann, Claudia Angela Maziero Volpato. Impact of laboratory treatment with coloring and fluorescent liquids on the optical properties of zirconia before and after accelerated aging // The Journal of Prosthetic Dentistry. - 2018;120:276-281. DOI: 10.1016/j.prosdent.2017.10.017 Дьяконенко Е.Е., Вердиян С.А., Сахабиева Д.А., Лебеденко И.Ю. Флуоресценция стоматологических керамических материалов на основе диоксида циркония. Стоматология. 2021;100(3):109-114. [E.E. Dyakonenko, S.A. Verdiyan, D.A. Sakhabieva, I.Yu. Lebedenko. Fluorescence of zirconia-based dental ceramic materials. Dentistry. 2021;100(3):109-114. (In Russ.)]. https://doi.org/10.17116/stomat2021100031109 D'yakonenko E.E., Verdiyan S.A., Sahabieva D.A., Lebedenko I.Yu. Fluorescenciya stomatologicheskih keramicheskih materialov na osnove dioksida cirkoniya. Stomatologiya. 2021;100(3):109-114. [E.E. Dyakonenko, S.A. Verdiyan, D.A. Sakhabieva, I.Yu. Lebedenko. Fluorescence of zirconia-based dental ceramic materials. Dentistry. 2021;100(3):109-114. (In Russ.)]. https://doi.org/10.17116/stomat2021100031109 Monsénégo G., Burdairon G., Clerjaud B. Fluorescence of dental porcelain // J Prosthet Dent. - 1993;69(1):106-113. doi:10.1016/0022-3913(93)90249-n Monsénégo G., Burdairon G., Clerjaud B. Fluorescence of dental porcelain // J Prosthet Dent. - 1993;69(1):106-113. doi:10.1016/0022-3913(93)90249-n Горбань С.А., Михалева Е.А., Полтанов В.Н., Степкин В.И., Чуев В.П. Воссоздание эффекта флуоресценции в стоматологической керамике «Ультропалин». Современная ортопедическая стоматология. 2014;21:71-74. [S.A. Gorban, E.A. Mikhaleva, V.N. Poltanov, V.I. Stepkin, V.P. Chuev. Reconstruction of the fluorescence effect in dental ceramics "Ultropalin". Modern orthopedic dentistry. 2014;21:71-74. (In Russ.)]. https://vladmiva.ru/publications/vossozdanie-effekta-fluorestsentsii-v-stomatologicheskoy-keramike-ultropalin/ Gorban' S.A., Mihaleva E.A., Poltanov V.N., Stepkin V.I., Chuev V.P. Vossozdanie effekta fluorescencii v stomatologicheskoy keramike «Ul'tropalin». Sovremennaya ortopedicheskaya stomatologiya. 2014;21:71-74. [S.A. Gorban, E.A. Mikhaleva, V.N. Poltanov, V.I. Stepkin, V.P. Chuev. Reconstruction of the fluorescence effect in dental ceramics "Ultropalin". Modern orthopedic dentistry. 2014;21:71-74. (In Russ.)]. https://vladmiva.ru/publications/vossozdanie-effekta-fluorestsentsii-v-stomatologicheskoy-keramike-ultropalin/ Takahashi M.K., Vieira S., Rached R.N., de Almeida J.B., Aguiar M., de Souza E.M. Fluorescence intensity of resin composites and dental tissues before and after accelerated aging: a comparative study // Oper Dent. - 2008;33(2):189-195. doi:10.2341/07-74 Takahashi M.K., Vieira S., Rached R.N., de Almeida J.B., Aguiar M., de Souza E.M. 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